Multiresidue analysis of four pesticide residues in water dropwort (Oenanthe javanica)via pressurized liquid extraction, supercritical fluid extraction, and liquid–liquid extraction and gas chromatographic determination
نویسندگان
چکیده
منابع مشابه
Comparisons of soxhlet extraction, pressurized liquid extraction, supercritical fluid extraction and subcritical water extraction for environmental solids: recovery, selectivity and effects on sample matrix.
Extractions of a polycyclic aromatic hydrocarbon (PAH)-contaminated soil from a former manufactured gas plant site were performed with a Soxhlet apparatus (18 h), by pressurized liquid extraction (PLE) (50 min at 100 degrees C), supercritical fluid extraction (SFE) (1 h at 150 degrees C with pure CO2), and subcritical water (1 h at 250 degrees C, or 30 min at 300 degrees C). Although minor diff...
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Multiple pesticide residues have been observed in some samples of canned foods, frozen vegetables, and fruit jam, which put the health of the consumers at risk of adverse effects. It is quite apparent that such a state of affairs calls for the need of more accurate, cost-effective, and rapid analytical techniques capable of detecting the minimum concentrations of the multiple pesticide residues...
متن کاملDetermination of pesticide residues in nonfatty foods by supercritical fluid extraction and gas chromatography/mass spectrometry: collaborative study.
A collaborative study was conducted to determine multiple pesticide residues in apple, green bean, and carrot by using supercritical fluid extraction (SFE) and gas chromatography/mass spectrometry (GC/MS). Seventeen laboratories from 7 countries participated in the final study, and a variety of different instruments was used by collaborators. The procedure simply entails 3 steps: (1) mix 1.1 g ...
متن کاملTrace analysis of explosives in soil: pressurized fluid extraction and gas and liquid chromatography-mass spectrometry.
Soil samples are collected from the former Open Burn/Open Detonation Unit, Makua Military Reservation, on the island of Oahu, Hawaii. The soil is the Helemano series. The soil samples are fortified with eight explosives for development of the analytical method. These analytes are 2-amino-4,6-dinitrotoluene; 1,3-dinitrobenzene; 2,4-dinitrotoluene (DNT); hexahydro-1,3,5-trinitro-1,3,5-triazine (R...
متن کاملDetermination of tetracycline residues in soil by pressurized liquid extraction and liquid chromatography tandem mass spectrometry.
An optimized extraction and cleanup method for the analysis of chlortetracycline (CTC), doxycycline (DC), oxytetracycline (OTC) and tetracycline (TC) in soil is presented. Soil extraction in a pressurized liquid extraction system, followed by extract clean up using solid-phase extraction (SPE) and tetracycline determination by liquid chromatography tandem mass spectrometry (LC-MS/MS) provided a...
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ژورنال
عنوان ژورنال: Journal of Separation Science
سال: 2007
ISSN: 1615-9306,1615-9314
DOI: 10.1002/jssc.200790047